Workflow
复合肥料
icon
Search documents
超高效液相色谱-串联质谱法测定复合肥料中乙烯利残留量
仪器信息网· 2025-10-03 03:58
Core Viewpoint - The article presents a novel method for detecting ethephon residues in compound fertilizers using Ultra-High-Performance Liquid Chromatography-Tandem Mass Spectrometry (UHPLC-MS/MS), addressing the lack of standardized methods for fertilizer matrices and providing a reliable technical foundation for regulatory monitoring and quality control [2][4][42]. Group 1: Method Development - A new UHPLC-MS/MS method was established to detect ethephon residues in compound fertilizers, optimizing key parameters based on SN/T 4522-2016 [4][7]. - The method replaced alkaline elution with an acidified extraction system (acetonitrile-0.1% formic acid), improving recovery rates from undetectable levels to 93.8%-104.5% [4][6]. - The method demonstrated excellent linearity (r=0.9993) within a range of 2-200 μg/L, with a quantitation limit of 0.005 mg/kg and relative standard deviation (RSD) of 1.3%-3.9% [4][29]. Group 2: Importance of Ethephon in Fertilizers - Ethephon is often added to fertilizers to enhance crop growth and development, but its presence raises concerns regarding potential residues in agricultural products [5][6]. - The complexity of compound fertilizers, which contain multiple nutrients and additives, necessitates effective monitoring of ethephon to ensure safety and compliance [5][7]. Group 3: Practical Application and Results - Actual sample testing revealed ethephon residues in commercial compound fertilizers, with detected levels of 0.008 mg/kg and 0.015 mg/kg in two batches [39][41]. - The study emphasizes the need for regulatory frameworks to monitor ethephon residues in fertilizers, highlighting the method's practical applicability for ensuring agricultural safety [42].
河南省鹤壁市市场监督管理局公布安全帽等16种产品质量监督抽查结果
Summary of Key Points Core Viewpoint The recent quality supervision inspection conducted by the Hebi City Market Supervision Administration in Henan Province revealed that out of 213 batches of products sampled, 10 batches failed to meet quality standards, highlighting concerns regarding product safety and compliance in the local market. Group 1: Inspection Overview - The inspection covered 16 types of products, including safety helmets, compound fertilizers, student stationery, toys, and electrical cables [1][2] - A total of 120 business entities were sampled during the inspection [1] Group 2: Compliance and Non-compliance - Out of the 213 batches tested, 203 batches were found to comply with the standards, while 10 batches were identified as non-compliant [2] - The non-compliant products included 4 batches of finished oil, 2 batches of safety helmets, 1 batch of compound fertilizer, 1 batch of reading glasses, 1 batch of student stationery, and 1 batch of electrical cables [2] Group 3: Action Taken - The Hebi City Market Supervision Administration has mandated relevant county (district) market supervision departments to handle the issues identified during the inspection according to applicable laws and regulations [2] - Cases involving production units located in other regions have been forwarded to the appropriate market supervision departments for investigation and handling [2]
山东对肥料生产企业进行“体检”
Da Zhong Ri Bao· 2025-08-18 01:01
Core Points - The provincial agricultural and rural department has initiated a "double random, one public" supervision inspection of fertilizer production enterprises starting from mid-August, aiming to purify the fertilizer production and operation market and ensure agricultural production and product quality safety [1] - The inspection will conclude by the end of October and targets organic fertilizers, organic-inorganic compound fertilizers, and compound fertilizers, with a minimum of 30% of marked enterprises being inspected, totaling no less than 183 companies [1] - The inspection will cover whether products have obtained fertilizer registration certificates, if there are any expired, counterfeit, or rented certificates, whether technical indicators match the registration certificate, compliance of packaging labels with regulations, and if production conditions meet the requirements of registered products [1] - Results of the inspections will be recorded in the regulatory platform and publicly disclosed in the National Enterprise Credit Information Publicity System (Shandong) [1]
南京市市场监管局发布复混肥料产品抽查结果
Core Viewpoint - The Nanjing Municipal Market Supervision Administration has released the results of the first batch of product quality supervision and inspection for 2025, indicating that all 20 batches of mixed fertilizers tested were found to be compliant with quality standards [1]. Group 1: Product Quality Inspection Results - A total of 20 batches of mixed fertilizers were sampled and all were found to be qualified [1]. - The inspection covered various types of mixed fertilizers, including organic-inorganic and compound fertilizers, with specifications ranging from 5kg to 50kg per bag [2][3]. - Specific brands such as "地得益," "肥地丰," and "宁粮" were among those tested, all receiving a compliance rating [2][3]. Group 2: Administrative Oversight - The inspection was conducted by the Nanjing Municipal Market Supervision Administration, emphasizing the importance of product quality in the agricultural sector [1]. - The results reflect the effectiveness of regulatory measures in ensuring that agricultural products meet safety and quality standards [1].
安徽省安庆市市场监督管理局公示2025年产品质量监督抽查结果(第三批)
| 索 引 号: | 78/202508-00004 | 信息分类: | 监督检查信息 | | --- | --- | --- | --- | | 文 号: | | 是否有效 : | 有效 | | 发布机构: | 安庆市市场监督管理局 | 成文日期: | | | 生效日期: | | 废止日期: | | | 主題分类: | | 体裁分类: | | | 服务对象: | | 生命周期: | | | 关键词: | | 发文日期: | 2025-08-05 09:59 | | 名 称: | 安庆市市场监督管理局2025年产品质量监督抽查结果公示(第三批) | | | | 10 生 | 铜芯聚氯乙烯绝 | 横电 | BVVB 2×2.5mm^(2) | 2025.6.5 | 安庆横电电缆有 | 安庆横电电缆有 | 是 | / | 皖西南产 | | --- | --- | --- | --- | --- | --- | --- | --- | --- | --- | | 产 | 缘聚氯乙烯护套 | 电缆 | | | 限公司 | 限公司 | | | 品质量 监 | | | 扁形电缆 | | | | | | | | 督检验中 ...
内蒙古巴彦淖尔市市场监督管理局发布2025年第一批产品质量监督抽查结果
Core Viewpoint - The Inner Mongolia Bayannur Market Supervision Administration has released the first batch of product quality supervision and spot check results for 2025, focusing on agricultural materials during the spring farming preparation period, including polyethylene blown agricultural ground cover films, drip irrigation belts, and fertilizers [3]. Group 1: Product Quality Results - A total of 170 batches of products were inspected, with 164 batches passing and 6 batches failing the quality tests [3]. - The non-compliant items included polyethylene blown agricultural ground cover films, which failed on thickness, tensile load, and tear resistance; drip irrigation belts, which failed on tensile performance and flow uniformity; and fertilizers, which failed on total nutrient content [3]. Group 2: Inspection Details - The inspection covered various products such as polyethylene blown agricultural ground cover films, single-wing labyrinth drip irrigation belts, inner embedded drip irrigation belts, urea, compound fertilizers, diammonium phosphate, potassium fertilizers, large (medium) soluble fertilizers, and microbial agents [3]. - The inspection was conducted randomly across different banners and counties in Bayannur City [3].
圣泉集团: 圣泉集团公司章程
Zheng Quan Zhi Xing· 2025-06-30 16:11
General Provisions - The company aims to protect the legal rights of the company, shareholders, and creditors, and to regulate its organization and behavior according to relevant laws and regulations [1][2] - The company was established as a joint-stock limited company based on the overall restructuring of Jinan Shengquan Chemical Industry Co., Ltd. and was approved by local economic reform committees [2][3] - The company was approved by the China Securities Regulatory Commission for its initial public offering of 81.06 million shares on July 8, 2021, and was listed on the Shanghai Stock Exchange on August 10, 2021 [3][4] Company Structure - The registered capital of the company is RMB 846,401,998 [2][3] - The company is a permanent joint-stock limited company, with the chairman serving as the legal representative [3][4] - The company's assets are divided into equal shares, and shareholders are liable for the company's debts only to the extent of their subscribed shares [3][4] Business Objectives and Scope - The company's business objectives include market-oriented management, systematic technological development, rational production organization, and maximizing shareholder interests [4][5] - The approved business scope includes the research, production, and sales of various chemical products, including furan resin and cold core box resin, as well as power generation and various types of fertilizers [5][6] Share Issuance - The company issues shares in the form of stocks, with each share having a par value of RMB 1 [6][7] - The initial issuance consisted of 14.65 million shares, with 11.27 million shares (76.9%) subscribed by Jinan Shengquan Industrial Co., Ltd. and 3.38 million shares (23.1%) subscribed by internal employees [7][8] - The total number of shares issued by the company is 846,401,998, all of which are ordinary shares [7][8] Shareholder Rights and Responsibilities - Shareholders have rights to dividends, participate in shareholder meetings, supervise company operations, and request information [11][12] - Shareholders are obligated to comply with laws and regulations, pay their subscribed capital, and not abuse their rights to harm the company or other shareholders [13][14] - Major shareholders (holding over 5% of shares) must report any pledges of their shares to the company [14][15] Shareholder Meetings - The company holds annual and temporary shareholder meetings, with the annual meeting occurring within six months after the end of the previous fiscal year [45][46] - Shareholder meetings are the company's decision-making body, responsible for approving major company decisions, including business plans and financial reports [40][41] - The company must provide adequate notice of meetings, including details on the agenda and voting procedures [57][58] Voting and Resolutions - Resolutions at shareholder meetings can be ordinary or special, with ordinary resolutions requiring a simple majority and special resolutions requiring a two-thirds majority [78][79] - Shareholders can exercise their voting rights based on the number of shares they hold, with each share granting one vote [80][81] - Related shareholders must abstain from voting on matters that involve their interests to ensure fair decision-making [30][31]
陕西省子长市市场监督管理局发布36批次产品检验情况通告
Summary of Key Points - The Shaanxi Zichang Market Supervision Administration conducted a quality inspection of 36 batches of products, with 32 passing and 4 failing [2][4][5] - The inspection covered various product categories, including electrical wires and fertilizers, indicating a focus on essential consumer goods [3][4] - The detailed inspection results are available in an attached summary table, which lists the specific products, manufacturers, and inspection outcomes [5][6]
辽宁省大连市市场监督管理局通报2025年化肥、农用薄膜等产品质量监督抽查情况
Overall Inspection Results - The inspection covered 13 product categories with a total of 200 batches, including fertilizers, agricultural films, plastic shopping bags, agricultural machinery, and more [3] - A total of 48 production enterprises and 131 distribution units were inspected, with 1 batch from a production enterprise and 12 batches from distribution units found to be non-compliant [3] Fertilizers - The inspection of fertilizers followed national standards such as GB/T 15063-2020 and GB/T 21633-2020, and no non-compliant products were found [4] Agricultural Films - The inspection of agricultural films revealed non-compliance in thickness and thickness deviation, based on standards GB 13735-2017 and GB/T 4455-2019 [4] Plastic Shopping Bags - Non-compliance was found in environmental requirements and thickness for plastic shopping bags, inspected under GB/T 21661-2020 and GB/T 38082-2019 [4] Agricultural Machinery - No non-compliance was detected in agricultural machinery, inspected according to JB/T 9822.1-2018 and JB/T 10749-2018 [5] Agricultural Submersible Pumps - The inspection of agricultural submersible pumps showed no non-compliance, following GB/T 25409-2010 and GB/T 2816-2014 standards [5] Fire Emergency Lighting - All fire emergency lighting products passed inspection, adhering to GB 17945-2010 standards [5] Fire Hoses - Fire hoses were compliant with GB 6246-2011 standards, with no non-compliance found [6] Fire Doors - Fire doors passed inspection based on GB 12955-2008 standards, with no issues reported [6] Electric Blankets - Electric blankets were compliant with GB 4706.1-2005 and GB 4706.8-2008 standards, showing no non-compliance [6] Indoor Heaters - Indoor heaters had issues with input power and current, as well as grounding measures, based on GB 4706.1-2005 and GB 4706.23-2007 standards [7] Down Jackets - No non-compliance was found in down jackets, inspected under GB/T 14272-2021 and GB 18401-2010 standards [7] Fireworks - Fireworks showed non-compliance in stability and ignition device components, based on GB 19593-2015 and GB 10631-2013 standards [8] Commodity Coal - All inspected commodity coal products were compliant with the relevant standards [9] Non-Compliant Enterprises - A list of non-compliant enterprises was provided, detailing specific products and non-compliance issues [10] Compliant Enterprises - A list of compliant enterprises was also provided, indicating that no issues were found during the inspection [11]
湖北化肥产品质量抽查合格率98.72%   
Zhong Guo Hua Gong Bao· 2025-05-26 02:17
Group 1 - The core viewpoint of the article highlights the results of the quality supervision inspection of fertilizer products conducted by the Hubei Provincial Market Supervision Administration, revealing a low non-compliance rate of 1.28% among the tested samples [1][2] - A total of 222 production and sales units were inspected, with 390 batches of fertilizers tested, of which 5 batches were found to be non-compliant [1][2] - The inspection covered various types of fertilizers, including compound fertilizers, mixed fertilizers, phosphate fertilizers, and organic fertilizers, with specific focus on parameters such as total nitrogen, effective phosphorus content, and potassium oxide [2] Group 2 - The inspection identified 4 batches of compound fertilizers from 4 production and sales units that did not meet quality standards, with issues related to total nitrogen, effective phosphorus content, and other key parameters [2] - The report emphasizes the need for local market supervision departments to enhance follow-up actions based on the inspection results, including recording the handling of issues in the Hubei Provincial Product Quality Supervision Management Information System [2] - It also calls for the enforcement of quality safety responsibilities among production and sales units, and the establishment of a risk management system to improve the overall quality level of the fertilizer industry [2]